9H-fluorene-2-carbaldehyde

CAS No. 30084-90-3

Formula: C14H10O
Basic Info

Formula
C14H10O
Molecular Weight
194.229
Exact Mass
194.073
LogP
3.0703
PSA
17.07
Synonyms

Fluorene-2-carbaldehyde

FLUORENE-2-CARBOXALDEHYDE

EINECS 250-035-2

2-Fluorenecarboxaldehyde

9H-fluorenyl-2-carbaldehyde

9H-Fluorene-2-carboxaldehyde

9H-fluoren-2-yl-carboxaldehyde

9H-2-fluorenecarboxaldehyde

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Properties
Appearance & Physical State
Sallow powder
Density
1.213g/cm3
Boiling Point
367.1ºC at 760mmHg
Melting Point
82-86ºC
Flash Point
232.5ºC
Refractive Index
1.681
Safety Info
RTECS
LL5917000
Safety Statements
S24/25
WGK Germany
3
Spectrum
NMR Spectrum 1H NMR : Predict
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Analysis Methods
Normal alkane RI, non-polar column, custom temperature program
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Column Shape
Capillary
Active Phase(℃)
Methyl Silicone
Retention index
1902.
Temperature Control
Method
custom temperature program
Comments
25. m/0.25 mm/0.25 μm, He; Program: 50 0C (2 min) <sup> </sup>20 0C/min -&gt; 160 0C <sup> </sup>5 0C/min -&gt; 210 0C <sup> </sup>10 0C/min -&gt; 300 0C
Reference
Oda, J.Yasuhara, A.Matsunaga, K.Saito, Y.Identification of polycyclic aromatic hydrocarbons of the particulate accumulated in the tunnel duct of freeway and generation of their oxygenated derivativesJpn. J. Toxicol. Environ. Health1998, 44, 5, 334-351.
Lee's RI, non-polar column, temperature ramp
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Column Shape
Capillary
Active Phase(℃)
HP-5
Retention index
292.7
Temperature Control
Method
temperature ramp
Comments
30. m/0.3 mm/0.25 μm, He, 50. C @ 5. min, 5. K/min, 200. C @ 15. min
Reference
Shao, X.Wang, G.Sun, Y.Zhang, R.Xie, K.Liu, H.Determination and Characterization of the Pyrolysis Products of Isoprocarb by GC-MSJ. Chromatogr. Sci.2006, 44, 3, 141-147.
Synthesis Route
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